Ionic Liquids as Green Solvents. Progress and Prospects by Robin D. Rogers, Kenneth R. Seddon PDF

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Extra info for Ionic Liquids as Green Solvents. Progress and Prospects

Sample text

Removal of water and ethanoic acid yielded 95 % of [dpeim][CH C0 ]. Ethanoic acid is a comparatively weak acid, and so the anion can easily be exchanged by an acid-base procedure as already described in Figure 1. - and S-[dpeim] salts with the following anions was prepared: triflate, chloride, bromide, iodide, nitrate, trifluoroethanoate, tetrafluoroborate and hexafluorophosphate. The acid was added to [dpeim][CH C0 ] and the aqueous solution extracted with dichloromethane. Evaporation of the solvent and drying in high vacuum yielded the corresponding chiral imidazolium salts.

Acta. 2000, 45, 1265-1270. Seddon, K. ; Torres, M-J. Pure Appl. Chem. 2000, 72, 22752287. ; ACS Symposium Series; American Chemical Society: Washington, DC, 2003. 30 15. 16. 17. ch002 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. 32. 33. 34. 35. 36. 37. 38. ; Dias, A. ; Kalyanasundaram, N . ; Grätzel, M . Inorg. Chem. 1996, 35, 1168-1172. ; Wasserscheid, P. German Patent DE 10003708, 2001. ; McCormac, P. B. Tetrahedron Lett. 1997, 38, 3097-3100. Earle, M . ; McCormac, P. ; Seddon, K. R.

21 (2001). 7. Wilkes, J. ; Zaworotko, M . , J. Chem. , Chem. Commun. 1992, 965. ; ACS Symposium Series; American Chemical Society: Washington, DC, 2003. ch004 3 Christine J. Bradaric , Andrew Downard *, Christine Kennedy , Allan J . O. com 1 2 3 4 5 Abstract While a great deal of attention has been given to imidazolium ionic liquids in recent years, very few investigations involving phosphonium ionic liquids have been reported in the open literature. Here we present an account of our research into ionic liquids from the perspective of a future, large-scale producer of ionic liquids for industrial applications.

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