By G.W. Parshall
ISBN-10: 0470131764
ISBN-13: 9780470131763
ISBN-10: 0470132469
ISBN-13: 9780470132463
The volumes during this carrying on with sequence offer a compilation of present innovations and concepts in inorganic man made chemistry. comprises inorganic polymer syntheses and training of significant inorganic solids, syntheses utilized in the advance of pharmacologically energetic inorganic compounds, small-molecule coordination complexes, and comparable compounds. additionally comprises worthy info on transition organometallic compounds together with species with metal-metal cluster molecules. All syntheses offered the following were confirmed.
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Additional resources for Inorganic Syntheses, Vol. 15
Example text
Phillips Petroleum Company, Research and Development Department, Bartlesville, Okla. 74004. Central Research Department, E. I. du Pont d e Nemours & Company, Wilmington, Del. 19898. ~ Procedure The reaction is carried out in an inert atmosphere using rigorously anhydrous solvent. , 5 mmoles) is added to 20 ml. 2 g. (11 mmoles) of methyldiphenylphosphine. The solid dissolves immediately, and within 1 minute, dark-red crystals begin to form. After 20 minutes the product is collected by filtration, washed twice with 8 ml.
Kondo, and A. , 90, 2278 (1968). 5. D. H. Gerlach, W. G. Peet, and E. L. , 94, 4545 (1972). 6. D. D. Titus, A. A. Orio, and H. B. Gray, Inorganic Syntheses, 13, 117 (1971). 7. J. J. Eisch and R. B. ), “Organometallic Syntheses,” vol. , New York, 1965; D. F. Shriver, “The Manipulation of Air-sensitive Compounds,” McGraw-Hill Book Company, New York. 1969. 12. TETRAHYDRIDOTETRAKIS(METHYLDIPHENYLPHOSPHINE)MOLYBDENUM(IV) [MoC14(p(CH3 } (C6H 5 12 2 1 + P(CH3 )(C6H 5 12 pz32H’ [MoH4(P(CH3)(C6H5), )41 Submitted by FILIPPO PENNELLA* Checkedby W.
6 A. BIS[ETHYLENEBIS(DIPHENYLPHOSPHINE)]DIHYDRIDOIRON(I1) Procedure Highly reactive anhydrous iron(I1) chloride is essential in this preparation. Iron(I1) chloride tetrahydrate may be dehydrated under vacuum or by azeotropic distillation. In either case the highly hygroscopic FeCl, must be protected from moist air before use. In vacuum drying, the FeCl,(H,O), is thoroughly ground under nitrogen anu is dried at 110" for 3-4 hours at ca. 1 torr in an Abderhalden pistol containing Drierite. In the azeotropic-distillation method, 50 g.
Inorganic Syntheses, Vol. 15 by G.W. Parshall
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